CRYSTAL STRUCTURE OF THE RUTHENIUM(II) NITROSOTRICHLORO COMPLEX Na[RuNOCl3(H2O)OH]·2H2O
V. A. Emel'yanov, I. A. Baidina, S. A. Gromilov
Keywords: ruthenium, nitroso complexes, chloro complexes, X-ray diffractometry, crystal chemistry
Pages: 342-347
Abstract
The crystal structure of the coordination compound Na[RuNOCl3(H2O)OH]·2H2O is reported. The complex is studied by IR and NMR spectroscopy, powder and single crystal X-ray diffraction. Crystallographic data determined for H7Cl3NNaO5Ru is: a = 6.648(2) Å, b = 8.216(7) Å, c = 10.063(3) Å, α = 89.75(6)°, β = 70.96(2)°, γ = 78.76(5)°, V = 967.9(2) Å3, P1 space group, Z = 4, dx = 2.165 g/cm3.
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